D5769_12
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Ensure that the
gas chromatographic
and mass spectrometer
operating conditions
are identical to those
used for calibration,
that the system is
properly calibrated,
and that all of the
criteria in Section 9 and 10
of the written standard are met.
Transfer a sufficient
quantity of the chilled sample
containing the appropriate
internal standards from Section
11 of the written standard to
fill a gas chromatographic auto
sampler vial and seal it
with a leak-free septum cap.
Place the sample vial
on the auto sampler
and start the analysis.